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ASTM D7948-14

Standard Test Method for Measurement of Respirable Crystalline Silica in Workplace Air by Infrared Spectrometry

1.1 This standard specifies a test method for collection and analysis of samples of airborne particulate matter for measurement of respirable crystalline silica by infrared (IR) spectrometry.

1.2 This test method is applicable to the analysis of crystalline silica (the polymorphs quartz, cristobalite and tridymite) over a working range of 0.025 to 0.4 mg/m3 for a 400 L air sample or 0.02 to 0.25 mg/m3 for a 1000 L air sample, depending on the analytical method.

1.3 The methodology is applicable to personal sampling of the respirable fraction of airborne particles and to static (area) sampling.

1.4 This test method describes three different procedures for sample preparation and infrared analysis of airborne crystalline silica samples, which are delineated in Annex A1 – Annex A3, respectively: (1) a potassium bromide (KBr) disc IR measurement method, (2) indirect IR analysis after redeposition onto a filter used for measurement, and (3) direct on-filter IR analysis.


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