NOTE Although MBTS is not a sulfenamide, it is the primary decomposition product of these accelerators and quantitatively determined by the method specified in 5.2.
The analytical methods are applicable for most commercial sulfenamide accelerators:
- sulfenamides of primary amines (type I);
- sulfenamides of unhindered secondary amines (type II);
- sulfenamides of hindered secondary amines (type III).
The method (5.2) to determine purity by high performance liquid chromatography (HPLC) is the preferred method.
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