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Other Wastewater Measurements

Standards for wastewater measurements address the standard test methods, guides, and practices for measuring turbidity, flow, and other properties of wastewater, as well as sampling. Given the focus on testing and measurement, standardization of this field of wastewater management has been greatly contributed to by the efforts of ASTM International, previously known as the American Society for Testing and Materials.

For standards addressing content testing, see our dedicated pages for element specific wastewater measurements, and bacteria, biodegradable content, and toxicity wastewater measurements.


ASTM D5172-91(2015)

Standard Guide for Documenting the Standard Operating Procedures Used for the Analysis of Water

1.1 This guide addresses the need for each laboratory engaged in the analysis of water and wastewater to develop and maintain an up-to-date written manual that clearly and completely delineates the exact steps followed in performing every test method and procedure used in the laboratory, that is, a manual of their standard operating procedures (SOPs). 1.2 This guide details the practices necessary to provide clear in-house SOPs and a mechanism whereby the normal development and evolution of an analytical test method or procedure can be controlled and properly evaluated for incorporation into the SOP used in that laboratory. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in the note.


ASCE/EWRI 2-06

Measurement of Oxygen Transfer in Clean Water

Measurement of Oxygen in Clean Water, ASCE/SEI 2-06, provides the latest methods for measuring the rate of oxygen transfer from diffused gas and mechanical oxygenation devices to water. A complete revision of ANSI/ASCE 2-91, this Standard represents the current consensus of the ASCE Committee on Oxygen Transfer Standards. ASCE/SEI 2-06 is applicable to laboratory scale oxygenation devices with water volumes of a few gallons as well as to full scale systems with water volumes typical of those found in the activated sludge wastewater treatment process. It is intended for use by engineers in the preparation of specifications for compliance testing and by manufacturers in the development of performance information.


ASTM D6238-98(2017)

Standard Test Method for Total Oxygen Demand in Water

1.1 This test method covers the determination of total oxygen demand in the range from 100 to 100 000 mg/L, in water and wastewater including brackish waters and brines (see 6.5 ). Larger concentrations, or samples with high suspended solids, or both, may be determined by suitable dilution of the sample. 1.1.1 Since the analysis is based on the change in oxygen reading of the carrier gas compared to that when a sample is introduced (see 4.1 ), the measurement range is a function of the amount of oxygen in the carrier gas. The higher the desired concentration range, the more oxygen required in the carrier gas. Under recommended conditions, the carrier gas concentration should be between two to four times the maximum desired oxygen demand. 1.1.2 The lower measurement range is limited by the stability of the baseline oxygen detector output. This signal is a function of the permeation system temperature, carrier gas flow rate, oxygen detector temperature, and reference sensor voltage. Combined, these variables limit the minimum recommended range to 2 to 100 mg/L. 1.1.3 The upper measurement range is limited by the maximum oxygen concentration in the carrier gas (100 %). With the recommended conditions of carrier gas concentration being two to four times the maximum oxygen demand, this limits the maximum possible oxygen demand to between 250 000 to 500 000 mg/L. However, as a practical application to water analysis, this test method will consider a maximum range of 100 000 mg/L. 1.2 This test method is applicable to all oxygen-demanding substances under the conditions of the test contained in the sample that can be injected into the reaction zone. The injector opening limits the maximum size of particles that can be injected. If oxygen-demanding substances that are water-insoluble liquids or solids are present, a preliminary treatment may be desired. These pretreatment methods are described in Annex A2 . 1.3 This test method is particularly useful for measuring oxygen demand in certain industrial effluents and process streams. Its application for monitoring secondary sewage effluents is not established. Its use for the monitoring of natural waters is greatly limited by the interferences defined in Section 6 . 1.4 In addition to laboratory analysis, this test method is applicable to on-stream monitoring. Sample conditioning techniques for solids pretreatment applications are noted in Annex A2 . 1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


ASTM D5879/D5879M-18

Standard Practice for Surface Site Characterization for On-Site Septic Systems

1.1 Site characterization of surface conditions at a site for evaluating suitability for on-site septic systems requires both simple and complex techniques that may be accomplished by many different procedures and may be variously interpreted. These studies are frequently site specific and are influenced by geological and geographical settings, by the purpose of the site characterization, by design requirements for the project proposed, and by the background, training, and experience of the staff involved. 1.2 This standard is a guide for using the surface site characterization for on-site septic systems method for projects that require on-site sewage disposal. It is intended to improve consistency of practice and to encourage the use of this method as part of a site characterization program. Since the subsurface conditions at a particular site are usually the result of a combination of natural, geologic, topographic, and climatic factors, and of historical modifications both natural and manmade, an adequate and internally consistent use of a method as part of the exploration program will allow evaluation of the results of these influences. 1.3 This practice can be used at any site where on-site treatment of residential and nonhazardous commercial wastewaters using septic tanks and natural soils or constructed filter beds is required or an option under consideration. This practice may also be useful when constructed wetlands are used as an alternative wastewater treatment method. 1.4 This practice should be used in conjunction with Practices D5921 and D5925 . 1.5 Units The values stated in either SI units or inch-pound units given in brackets are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of results in units other than SI shall not be regarded as nonconformance with this standard. 1.6 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project's many unique aspects. The word Standard in the title of this document means only that the document has been approved through the ASTM consensus process. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


ASTM D5091-95(2014)

Standard Guide for Water Analysis for Electrodialysis/Electrodialysis Reversal Applications

1.1 This guide covers the determinations that should be performed on any given water if processing by electrodialysis/electrodialysis reversal is being considered. 1.2 This guide is applicable to all waters but is not necessarily complete for wastewaters. 1.3 This is a guide only and should not be construed as a complete delineation of all analysis required for a specific application. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


ASTM D7243-11(2020)

Standard Guide for Measuring the Saturated Hydraulic Conductivity of Paper Industry Sludges

1.1 Paper industry sludges are industrial by-products derived from wastewater treatment operations at plants associated with the manufacturing of paper. These sludges typically consist of clay and organic matter. They may also contain low levels of inorganic and organic contaminants and can be rich in microbes. Traditionally, paper industry sludges have been disposed in municipal solid waste landfills or solid waste monofills. However, in the interest of sustainability, applications are being developed where sludges can be used beneficially. One application is using sludge to construct hydraulic barriers (for example, for use in a landfill cap). Such applications generally require that the hydraulic conductivity of the sludge be measured. 1.2 Compacted paper industry sludges generally behave like soils and are amenable to geotechnical testing methods. However, several of their attributes require special attention during testing. Compacted industry sludges generally are highly compressible due to their organic component. Thus, their hydraulic conductivity can be more sensitive to the effective stress and hydraulic gradient applied during testing than most soils. The microbes in paper sludge can also produce gas during testing, confounding testing methods. 1.3 This guide is intended to supplement ASTM D5084 , Test Methods for Measurement of Hydraulic Conductivity of Saturated Porous Materials Using a Flexible Wall Permeameter. The purpose of the guide is to provide additional guidance on issues relevant to testing sludges using Test Methods D5084 . The guide applies to specimens compacted in the laboratory using procedures such as those described in Test Methods D698 and D1557 or undisturbed specimens collected from the field using procedures such as Practice D1587/D1587M or Practice D7015/D7015M . 1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. This standard contains a hazards section regarding the use of biocides (Section 10 ). 1.6 This guide offers an organized collection of information or a series of options and does not recommend a specific course of action. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this guide may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project s many unique aspects. The word Standard in the title of this document means only that the document has been approved through the ASTM consensus process. 1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


ASTM D3977-97(2019)

Standard Test Methods for Determining Sediment Concentration in Water Samples

1.1 These test methods cover the determination of sediment concentrations in water and wastewater samples collected from lakes, reservoirs, ponds, streams, and other water bodies. In lakes and other quiescent-water bodies, concentrations of sediment in samples are nearly equal to concentrations at sampling points; in most instances, sample concentrations are not strongly influenced by collection techniques. In rivers and other flowing-water bodies, concentrations of sediment in samples depend upon the manner in which the samples are collected. Concentrations in isokinetically-collected samples can be multiplied by water discharges to obtain sediment discharges in the vicinity of the sampling points. 1.2 The procedures given in these test methods are used by the Agricultural Research Service, Geological Survey, National Resources Conservation Service, Bureau of Reclamation, and other agencies responsible for studying water bodies. These test methods are adapted from a laboratory-procedure manual 2 and a quality-assurance plan. 3 1.3 These test methods include: 1.4 Test Method A can be used only on sediments that settle within the allotted storage time of the samples which usually ranges from a few days to a few weeks. A correction factor must be applied if dissolved-solids concentration exceeds about 10 % of the sediment concentration. 1.5 Test Method B can be used only on samples containing sand concentrations less than about 10 000 ppm and clay concentrations less than about 200 ppm. The sediment need not be settleable because filters are used to separate water from the sediment. Correction factors for dissolved solids are not required. 1.6 Test Method C can be used if two concentration values are required: one for sand-size particles and one for the combination of silt and clay-size particles. The silt-clay fraction need not be settleable. 1.7 These test methods must not be confused with turbidity measurements discussed in Test Method D1889 . Turbidity is the optical property of a sample that causes light rays to be scattered and absorbed; it is not an accurate measure of the mass or concentration of sediment in the sample. 1.8 These test methods contain some procedures similar to those in Methods of Test D1888 which pertains to measuring particulate and dissolved matter in water. 1.9 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. 1.11 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


ASTM D5463-18

Standard Guide for Use of Test Kits to Measure Inorganic Constituents in Water

1.1 This guide covers general considerations for the use of test kits for quantitative determination of analytes in water and wastewater. Test kits are available from various manufacturers for the determination of a wide variety of analytes in drinking water, surface or ground waters, domestic and industrial feedwaters and wastes, and water used in power generation and steam raising. See Table 1 for a listing of some of the types of kits that are available for various inorganic analytes in water. 2 (A) Kit Methodology: A = appearance/turbidity, C = visual colorimetric, GNG = go no go, P = photometric, and T = titrimetric. 1.2 Ranges, detection limits, sensitivity, accuracy, and susceptibility to interferences vary from kit to kit, depending on the methodology selected by the manufacturer. In some cases, kits are designed to replicate exactly an official test method of a standard-setting organization such as the Association of Official Analytical Chemists (AOAC), American Public Health Association (APHA), ASTM, or the U.S. Environmental Protection Agency (USEPA). In other cases, minor modifications of official test methods are made for various reasons, such as to improve performance, operator convenience, or ease of use. Adjustments may be made to sample size, reagent volumes and concentrations, timing, and details of the analytical finish. In yet other cases, major changes may be made to the official test method, such as the omission of analytical steps, change of the analytical finish, omission of reagents, or substitution of one reagent for another. Reagents in test kits are often combined to obtain a fewer number and make the test easier to use. Additives may also be used to minimize interferences and to make the reagent more stable with time. A kit test method may be based on a completely different technology, not approved by any official or standard-setting organization. Combinations of test kits multi-parameter test kits may be packaged to satisfy the requirements of a particular application conveniently. The test kits in such combination products may be used to make dozens of determinations of several parameters. 1.3 Test kit reagent refills are commonly available from manufacturers. Refills permit cost savings through reuse of the major test kit components. 1.4 Because of the wide differences among kits and methodologies for different analytes, universal instructions cannot be provided. Instead, the user should follow the instructions provided by the manufacturer of a particular kit. 1.5 A test kit or kit component should not be used after the manufacturer's expiration date; it is the user's responsibility to determine that the performance is satisfactory. 1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 10 . 1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


ASTM D4309-18

Standard Practice for Sample Digestion Using Closed Vessel Microwave Heating Technique for the Determination of Total Metals in Water

1.1 This practice covers the general considerations for quantitative sample digestion for total metals in water using closed vessel microwave heating technique. This practice is applicable to surface, saline, domestic, and industrial wastewater. 1.2 Because of the differences among various makes and models of satisfactory instruments, no detailed operating instructions can be provided. Instead, the analyst should follow the instructions provided by the manufacturer of the particular instrument. 1.3 This practice can be used with the following ASTM standards, providing the user determines precision and bias based on this digestion practice: Test Method D857 , Test Methods D858 , Test Methods D1068 , Test Methods D1687 , Test Methods D1688 , Test Methods D1691 , Test Methods D1886 , Test Method D1976 , Practices D3370 , Test Methods D3557 , Test Methods D3559 , Practice D3919 , Test Method D4190 , Practice D4453 , Practice D4691 , and Test Method D5673 . 1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversion to inch-pound units that are provided for information only and are not considered standard. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9 . 1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


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