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ASTM D7151-15

Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

1.1 This test method describes the determination of metals and contaminants in insulating oils by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1. This test method is similar to Test Method D5185, but differs in methodology, which results in the greater sensitivity required for insulating oil applications.

1.2 This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine insoluble particulates. Analytical results are particle size dependent, and low results are obtained for particles larger than several micrometers.2

1.3 This test method determines the dissolved metals (which can originate from overheating or arcing, or both) and a portion of the particulate metals (which generally originate from a wear mechanism). While this ICP method detects nearly all particles less than several micrometers, the response of larger particles decreases with increasing particle size because larger particles are less likely to make it through the nebulizer and into the sample excitation zone.

1.4 This test method includes an option for filtering the oil sample for those users who wish to separately determine dissolved metals and particulate metals (and hence, total metals).

1.5 Elements present at concentrations above the upper limit of the calibration curves can be determined with additional, appropriate dilutions and with no degradation of precision.

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